Sample Preparation
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Sample Preparation for ICP Analysis
Running ICP samples is fairly straightforward, although attention to detail while setting up the samples is very important. Click here for a write-up for running the ICP-OES.
The most critical part of obtaining reliable data is sample preparation. This cannot be overemphasized!
There is an excellent website produced by Inorganic Ventures, INC., of Lakewood, NJ, that gives a huge amount of useful information on just about everything you need to know. You are strongly advised to check this website before you start sample preparation.
Here are links to some really useful items on their website:
Periodic Table
http://www.inorganicventures.com/extras/pertable/
Reliable Measurements
A Guidebook for Trace Analysis
http://www.inorganicventures.com/tech/reliability/
ICP Operations
A Guide for New ICP Users
http://www.inorganicventures.com/tech/icp-ops/
Sample Preparation Guide
Considerations in the Preparation of Elemental Chemical Solutions